Magnetic Solid Phase Extraction based on Amino-functionalized Magnetic Starch for Analysis of Organochlorine Pesticides
نویسندگان
چکیده
منابع مشابه
Synthesis and Application of Novel Modified Magnetic Nanocomposite for Solid Phase Extraction of Thallium(I) Ions
In this paper, magnetically multiwalled carbon nanotubes (MMWCNTs) nanocomposite modified by methyl-2-[2-(2-2-[2-(methoxycarbonyl) phenoxy] ethoxyethoxy) ethoxy] benzoate was applied for magnetic solid-phase extraction (MSPE) of thallium(I) ions. Fourier transform infrared (FT-IR) spectroscopy, field emission scanning electron microscopy (FE-SEM), X-ray diffraction (XRD) spectrometry and vibrat...
متن کاملSolid-phase extraction method for the quantitative analysis of organochlorine pesticides in wildlife urine.
A gas chromatographic method for the analysis of nine organochlorine pesticides in wildlife urine is described. Reversed-phase solid-phase extraction is utilized to extract the organochlorine pesticides from urine. The pesticides are recovered by elution with hexane-ethyl ether (1:1) and quantified by gas chromatography with electron-capture detection. Method detection limits range from 1.4 to ...
متن کاملDetermination of Lead and Cadmium in Various Food Samples by Solid Phase Extraction Using a Novel Amino-Vinyl Functionalized Iron Oxide Magnetic Nanoparticles
A facile method for synthesis of amino functionalized silica coated Fe3O4 magnetic nanoparticles is introduced. For this purpose, the surface of magnetic nanoparticles (MNPs) was modified with two precursors of silica which produced amine and vinyl functional groups on the surface of magnetic nanoparticles. The modified magnetic nanoparticles were characterized by transmission electron micr...
متن کاملSolid Phase Extraction Using Modified Magnetic Iron Oxide Nanoparticles for Extraction and Spectrofluorimetric Determination of Carvedilol in Human Plasma Samples
A new analytical approach was developed involving magnetic solid–phase extraction and spectrofluorimetric determination of carvedilol in human plasma samples. A plasma sample was prepared and adjusted to pH 8.2–10, then carvedilol was quickly extracted using iron oxide magnetic nanoparticles modified by the surfactant cetyltrimethylammonium bromide and determined to apply spectrofluorimetry...
متن کاملNovel Functionalized Polythiophene-Coated Fe3O4 Nanoparticles for Magnetic Solid-Phase Extraction of Phthalates
Poly(phenyl-(4-(6-thiophen-3-yl-hexyloxy)-benzylidene)-amine) (P3TArH) was successfully synthesized and coated on the surface of Fe3O4 magnetic nanoparticles (MNPs). The nanocomposites were characterized by Fourier transform infra-red (FTIR), X-ray diffractometry (XRD), Brunauer-Emmett-Teller (BET) surface area analysis, analyzer transmission electron microscopy (TEM) and vibrating sample magne...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ژورنال
عنوان ژورنال: Analytical Sciences
سال: 2021
ISSN: 0910-6340,1348-2246
DOI: 10.2116/analsci.21p034